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Аннотация This paper is devoted to study of aluminium agglomeration in the process of burning of solid rocket propellants. The paper describes methods of experimental study of agglomerate internal structure which provides receiving quantitative information about parameters of agglomerate structure and makes it possible to check hypotheses of agglomerate internal structure. Rather high quality of presented experimental technique has been confirmed by the results of conducted experimental studies. In combination with other methods of agglomeration study this technique is to allow us to develop more adequate description of the agglomeration process