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Опубликовано
2007-02-20
Опубликовано на SciPeople2009-07-23 11:24:17
ЖурналRadiation Measurements, 2007, vol. 42, pp. 708-711.
Luminescence, vibrational and XANES studies of AlN nanomaterials
Radiation Measurements, 2007, vol.42, pp. 708-711.
Аннотация
The paper reports comparative studies on synthesized aluminium nitride nanotubes, nanoparticles and commercially available micron-sized AlN powder using different spectroscopic techniques: cathodoluminescence measurements (CL), X-ray absorption near edge spectroscopy (XANES) and Fourier-transform infrared spectroscopy (FTIR). Crucial distinctions in CL spectra are observed for nano- and microsized aluminium nitride powders; systematic shift of the IR absorption maximum has been detected for nanostructured aluminium nitride as compared to commercial samples. Through XANES experiments on Al K-edge structural differences between nano- and bulk AlN are revealed, intensity of features in absorption spectra has been found to be a function of wurtzite and zincblend phases amount in nanostructured samples.
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